F-100L barrel type

Autonomous products and other conventional products


Classification:

Single-layer glass reactor


Key words: experimental instrument


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Product Details

Scientific instruments are tools for precision measurement, and their precision and reliability must be an order of magnitude higher than the object being measured. Therefore, although there are not as many components as airplanes, the systematic design is also beyond imagination. The chromatographic column, as a consumable, is a separation center, just like the heart. High pressure, tightness and flow rate stability are required. And the oven needs to be kept at a constant temperature. To prevent leakage, maintain constant temperature, pressurized flow, every link, can not be slack. For materials, seals, and fluid mechanics, a high foundation is required.

The method for checking whether the instrument leaks: pinch off the external vacuum skin tube, and observe whether the vacuum gauge on the instrument can keep the instrument leak-free for five minutes. If there is air leakage, check whether the sealing ring on each sealing joint and rotating shaft is effective. On the contrary, the instrument is normal to check the vacuum pump and vacuum pipeline.

F-100L single-layer cylindrical glass reactor

Model: F-100L

Features: F-100L single-layer cylindrical glass reactor has an electric constant speed stirring system, condensation, dropping system, and heating bath. While stirring the materials, the bath pot heats the materials in the kettle, which can improve the evaporation efficiency under vacuum conditions (to be connected with a vacuum device). The solvent vapor is cooled into liquid when passing through the glass condensing coil (to be connected with a cooling device), which can be returned to the kettle or recovered through the valve at the lower part of the reflux elbow. After the reaction is completed, the materials can be discharged from the side discharge port at the bottom of the kettle.

Working principle

This machine has electric constant speed stirring system, condensation, dropping system, heating bath pot. While stirring the materials, the bath pot heats the materials in the kettle, which can improve the evaporation efficiency under vacuum conditions (to be connected with a vacuum device). The solvent vapor is cooled into liquid when passing through the glass condensing coil (to be connected with a cooling device), which can be returned to the kettle or recovered through the valve at the lower part of the reflux elbow. After the reaction is completed, the materials can be discharged from the side discharge port at the bottom of the kettle.

This series of products need to be equipped with vacuum device, cooling circulation device and other system devices.

Basic configuration

• All parts in contact with the material are made of high borosilicate glass (expansion coefficient 3.3) and polytetrafluoroethylene material, which is stable and not easy to react with the material.

• The main bracket is made of cold plate anti-corrosion and plastic-sprayed aluminum alloy, and the pot liner is made of stainless steel

• Glass PTFE discharge valve, no liquid side discharge.

Low-speed booster motor, frequency conversion speed regulation, through the rotary fine adjustment, double display speed control box can digitally display the speed and the temperature of the material in the kettle.

• Thermostatic bath temperature digital display, with lock button switch control, pot bottom K-type sensor stainless steel probe.

The mixing system adopts ceramic bearing and mechanical seal to prevent the mixing rod from wearing off chips.

• Using PT100 temperature sensor, 304 stainless steel, transparent Teflon tube jacket, double anti-corrosion.

• Vacuum pressure gauge shows real-time vacuum, pointer display.

Crescent three-blade double-layer stirring paddle, 304 stainless steel PTFE stirring blade; The mixing rod is made of 304 stainless steel and is outsourced with PTFE tube.

The bottom of the pan is equipped with a water drain valve to facilitate liquid discharge.

• The bottom of the machine is equipped with a universal wheel with brake, which can move as a whole and is easy to operate.

• Stirring and heating double fuse safety protection.

Technical parameters

Model

F-100L

Capacity of kettle body

100L cylindrical Φ465mm inner length 696mm

Voltage frequency

Stirring 220V/50HZ heating pot 380V/50HZ

Stirring motor power

200W1/3

Heating power

8KW

Stirring speed

0-450rpm/min

Kettle body temperature range

-80 ℃ ~ 250 ℃

Temperature measurement accuracy

± 1 ℃

vacuum degree

0.098Mpa

 

 

kettle cover

Φ340mm six ports

Mixing port

Φ60mm flange port

Condensate return port

50# ball milling port

Constant pressure funnel mouth

40# mark

Decompression port

34# mark

Temperature measuring port

Φ45 flange port

Solid feeding port

Φ80mm flange port inner diameter Φ60mm matching PTFE cover

Stirring paddle

Φ17 × 1200H(mm) Leaf exhibition 240mm

Condenser size

Φ60 flange port under Φ120*600H(mm)

Condensation area

0.5 ㎡

Reflow elbow

Upper Φ60 flange port left 50# ball grinding plug lower 1L ball bottle with glass discharge valve

Constant pressure funnel capacity

2L upper 29# standard mouth with glass plug lower 40# standard plug

Pressure reducing valve

34# standard plug valve bleed nozzle (pagoda connector) outer diameter 12mm

discharge valve

Φ80 flange port Φ33mm discharge hole inclined discharge port (pagoda joint) Φ34mm 350mm from the ground

vacuum suction nozzle

External diameter of pagoda connector 12mm

Condensing coil inlet and outlet circulation nozzle

Outer diameter of pagoda joint 15mm

Pot gall size

Φ550 × 650H(mm)

Space size of the whole machine

900 × 770 × 2550mm wide, deep and high

machine net weight

110KG

Packing size

2050 × 690 × 1000mm wooden case 1.42m ³

Packing weight

163KG

F-100L barrel type

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