FT-150L

Autonomous products and other conventional products


Classification:

Explosion-proof double-layer glass reactor

Double glass reactor


Key words: experimental instrument


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Product Details

Scientific instruments are tools for precision measurement, and their precision and reliability must be an order of magnitude higher than the object being measured. Therefore, although there are not as many components as airplanes, the systematic design is also beyond imagination. The chromatographic column, as a consumable, is a separation center, just like the heart. High pressure, tightness and flow rate stability are required. And the oven needs to be kept at a constant temperature. To prevent leakage, maintain constant temperature, pressurized flow, every link, can not be slack. For materials, seals, and fluid mechanics, a high foundation is required.

The method for checking whether the instrument leaks: pinch off the external vacuum skin tube, and observe whether the vacuum gauge on the instrument can keep the instrument leak-free for five minutes. If there is air leakage, check whether the sealing ring on each sealing joint and rotating shaft is effective. On the contrary, the instrument is normal to check the vacuum pump and vacuum pipeline.

FT-150L double glass reactor

Model: FT-150L

Features: The FT-150L double-layer glass reactor has an electric constant speed stirring system, condensation and dropping system, and the interlayer of the kettle body needs to be externally connected with heating or cooling circulation equipment. While stirring the material, the circulating hot solution or cooling liquid is injected through the interlayer to heat or cool the material in the kettle at a constant temperature. When the material is heated, the evaporation efficiency can be improved under vacuum conditions (vacuum device needs to be connected). The solvent vapor is cooled into liquid when passing through the glass condensing coil (cooling device needs to be connected), which can be returned to the kettle or recovered through the valve at the lower part of the reflux elbow. After the reaction is completed, the materials can be discharged from the side discharge port at the bottom of the kettle.


Working principle

This machine has an electric constant speed stirring system, condensation and dropping system, and the sandwich of the kettle body needs external heating or cooling circulation equipment. While stirring the material, the circulating hot solution or cooling liquid is injected through the interlayer to heat or cool the material in the kettle at a constant temperature. When the material is heated, the evaporation efficiency can be improved under vacuum conditions (vacuum device needs to be connected). The solvent vapor is cooled into liquid when passing through the glass condensing coil (cooling device needs to be connected), which can be returned to the kettle or recovered through the valve at the lower part of the reflux elbow. After the reaction is completed, the materials can be discharged from the side discharge port at the bottom of the kettle.

This series of products use the need to support the vacuum device, high temperature or low temperature circulation device and other components of the system device.

Basic configuration

• All parts in contact with the material are made of high borosilicate glass (expansion coefficient 3.3) and PTFE materials, and the performance is stable and not easy to react with the material.

• Frame type body, made of aluminum alloy stainless steel.

• Glass PTFE discharge valve, no liquid side discharge.

Low-speed booster motor, frequency conversion speed regulation, through the rotary fine adjustment, double display speed control box can digitally display the speed and the temperature of the material in the kettle.

The mixing system adopts ceramic bearing and mechanical seal to prevent the mixing rod from wearing off chips.

• Using PT100 temperature sensor, 304 stainless steel, transparent Teflon tube jacket, double anti-corrosion.

• Vacuum pressure gauge shows real-time vacuum, pointer display.

Crescent double triple impeller three-layer stirring paddle, 304 stainless steel PTFE stirring blade; The stirring rod is made of 304 stainless steel and is covered with PTFE tube.

• The bottom of the machine is equipped with a universal wheel with brake, which can move as a whole and is easy to operate.

• Fuse safety protection.

Technical parameters

Model

FT-150L

Capacity of kettle body

150L inner diameter 550mm outer diameter 600mm inner length 786mm

Interlayer capacity

About 35L

Voltage frequency

220V/50HZ

Stirring motor power

750W1/5

Stirring speed

0-280rpm/min

Kettle body temperature range

-80 ℃ ~ 250 ℃

Temperature measurement accuracy

± 1 ℃

vacuum degree

0.098Mpa

 

 

kettle cover

Φ340mm

Six

Mixing port

Φ60mm flange port

Condensate return port

50# ball milling port

Dropping elbow mouth

50# ball milling port

Decompression port

34# mark

Temperature measuring port

Φ45mm flange port

Solid feeding port

Φ80mm flange port inner diameter Φ60mm matching PTFE cover

Stirring paddle

Φ20 × 1300H(mm) Leaf exhibition 240mm

Condenser

Φ60mm Flange under Φ160mm × 600H(mm)

Condensation area

0.95 ㎡

Reflow elbow

Upper Φ60 flange port left 50# ball grinding plug right 24# standard port with multi-function valve

Lower 50# ball mill plug valve

Dropping bottle

5L cylindrical upper 29# standard port is equipped with air release valve × 2 34# standard port is equipped with glass plug

Collection bottle

10L upper 50# ball milling port 24# standard port is equipped with bleed valve × 2 lower glass bleed valves

Pressure reducing valve

34# standard plug valve bleed nozzle (pagoda connector) outer diameter 12mm

Recirculating inlet and outlet of interlayer

Supporting flange plate and 6-minute outer wire adapter for Φ45mm flange opening

discharge port

Φ100mm flange Φ65mm discharge hole inclined discharge port (pagoda joint) Φ40mm 300mm from the ground

vacuum suction nozzle

External diameter of pagoda connector 12mm

Condenser coil inlet and outlet nozzle

Outer diameter of pagoda joint 15mm

Space size of the whole machine

1280 × 850 × 2730mm wide, deep and high

machine net weight

155KG

Packing size

2160 × 740 × 840mm 1360 × 750 × 850mm

Two wooden boxes 2.21m ³

Packing weight

271(159 112)KG

FT-150L

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